The Australian Wine Research Institute’s Analytical Service - Analyses

Agrochemical residue analysis

Multi residue assay (GCMS)

NATAlogo (16K)The Analytical Service provides a fast and reliable agrochemical residue analysis service to the Australian wine industry. The routine scan includes 33 residues, which include over 50 brand name agrochemicals. The analysis of wine and juice is accredited by the National Association of Testing Authorities (NATA) and is regularly exposed to international proficiency testing. Wherever possible, residues are analysed as per their maximum residue limit (MRL) definition.

An analytical method employing extraction, cleanup and gas chromatography/mass spectrometry (GC-MS) operating in selected ion monitoring mode has been developed for accurately determining the concentration of all of these compounds. The analysis can be used for any of the following matrices: grapes, wines, *leaves, juices, marc, *soil, water, *winery and vineyard effluent.

*Please call us if you would like these sample types analysed.

Multi residue assay (HPLC)

High pressure liquid chromatography (HPLC) with diode array detection is used for the determination of a number of residues not included in the MRA. These include Pyrimethanil, Fluidioxonil, Cyprodonil, Fenhexamid and Tebufenozide. This method is also NATA accredited for grapes, juice, wine and marc, and is exposed to international proficiency testing.

Strobilurins

The strobilurin analysis includes the recently registered azoxystrobin (both isomers), trifloxystrobin, pyraclostrobin and boscalid.

We also have validated methods for Emamectin, Fluazinam and Spinosad. Please contact us if you require these analyses.

For information regarding agrochemicals for use in the wine industry, please visit the agrochemicals web site or download the Institute publication, Agrochemicals registered for use in Australian viticulture 2005/2006 (0.7 MB PDF file).

The GCMS-MRA is currently being validated for tetraconazole and buprafezin, which have recently been registered for viticultural use.

Prices per sample (excluding GST)

Residue type

1-3 samples

4-7 samples

8+ samples

Multi residue assay (GC/MS) – wine or juice

$222

$180

$163

Multi residue assay (GC/MS) – grapes or marc

$271

$229

$206

Multi residue assay (HPLC) – wine

$175

$150

$136

Multi residue assay (HPLC) – grapes

$225

$198

$184

Carbendazim – wine or juice

$155

$126

$114

Carbendazim – grapes or marc

$216

$195

$173

Endosulfan

POA

Dithiocarbamates

$248

$201

$182

Strobilurins – wine or juice

$135

$125

$120

Strobilurins – grapes or marc

$211

$197

$190

2,4-D – wine

$245

$235

$226

2,4-D – grapes

$300

$288

$276

A handling fee of A$25 exclusive of GST applies per invoice.

Target response time - 10 working days from receipt of samples

Volume required: wine or juice - 500 mL

Quantity required: grapes or marc - 500 g

CRCV (1K)

The Australian Wine Research Institute uses a method developed as part of the collaborative research program of the Cooperative Research Centre for Viticulture.

For information regarding maximum residue levels for export destinations, please visit the Agrochemicals site.



Multi residue assay (GC-MS)

Agrochemical residues included in the assay:

Atrazine
Azinphos methyl
Benalaxyl
Captan
Carbaryl
Chlorothalonil
Chlorpyrifos
Chlorpyrifos methyl
Diazinon
Dicofol (both isomers)
Dimethoate
Dimethomorph

Ethion
Fenarimol
Fenitrothion
Fenthion
Flusilazole
Hexaconazole
Holoxacarb
Iprodione
Malathion
Metalaxyl
Methidathion
Myclobutinal

Oxadixyl
Parathion methyl
Penconazole
Procymidone
Propiconazole
Prothiophos
Quinoxyfen
Simazine
Spiroxamine
Tebuconazole
Triadimefon
Triadimenol
Vinclozolin